Special Organic Chemistry Lab II |
CHM 246 - Summer 2008 Mon-Tue-Thu 3:00 pm - 6:00 pm, AA429C |
Instructor: Dana Horoszewski, Ph.D. |
TEXT The linked webpages and douments in the table below are your text book for this course. If you want to supplement the information in the web pages, I reccomend The Organic Chem Lab Survival Manual: A Student's Guide to Techniques by James Zubrick (older editions available online for cheap) or Experimental Organic Chemistry: A Miniscale and Microscale Approach, by Gilbert & Martin (on reserve in the library) |
OTHER REQUIRED MATERIALS |
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| TENTATIVE LAB SCHEDULE |
| Date | Lab Activity | Lab Manual | Relevant Links |
| 6/24 | Check-In/Safety and Orientation | ||
| 6/26 | Computer Unknown | comp_unknown | |
| 6/30 | Computer Unknown Test | ||
| 7/1 | Wet Lab Unknown | wet_unknown | |
| 7/3 | Wet Lab Unknown | ||
| 7/7 | Begin Diels-Alder Cycloaddition | dielsalder | |
| 7/8 | Oxidation of Cyclohexanol | oxidation | |
| 7/10 | Grignard Reaction | grignard | |
| 7/14 | Finish Diels-Alder |
acid_base | |
| 7/15 | Self Assembled Monolayers | hydrophobic | |
| 7/17 | Synthesis of Apirin | aspirin | |
| 7/21 | Preparation of an Ester Begin Aldol Condensation |
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| 7/23 | Finish Aldol Condensation | ||
| 7/24 | Finish up Labs/Check out | ||
| 7/28 | No Lab | ||
| 7/29 | No Lab |
SOURCES OF INFORMATION This is a short list of where you may find the information required for this course. These are references where you might find densities, boiling points etc. for this lab: 1) Aldrich Chemical Catalog:This has the advantage of having many compounds in it, and listing them in alphabetical order.Watch out for grades of chemicals (Tech. 90% or ACS reagent grade 99.998%), and deuteration – addition of one or more deuterium atoms to replace hydrogen.The latter appears as, for example, “acetone-d 6”, or “ethyl acetate – d 3”.We will usually not use technical grade chemicals, and we never use isotopically substituted ones. 2) The Merck Index: Less comprehensive that Aldrich.Limited to chemicals that are biomedical in use.However, it is very readable. |